By Michael Dub (auth.), Michael Dub (eds.)
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Additional resources for Compounds of Arsenic, Antimony, and Bismuth: Covering the Literature from 1965 to 1968
Prepd. from [n-C~=C(Me)C~PdIJ2 + Ars in warm CeHe. NMR spectrum in CHC13 indicated a considerable dissocn. of the Ars ligand (1248). [rT-MeCH=CHC~Pd(Ars)ClJ, UV spectrum in CHC13 (717). [n-C~=CHCMe2Pd(Ars)ClJ, yellow prisms, m. ), prepd. from [n-C~=CHCMe2PdClJ2 + Ars in warm CeHe. IR and NMR spectra; asymmetric bond- ing of the allyl ligand postulated (l248). [n-Me2C=c(Me)C~Pd(Ars)ClJ, the formation of the complex from [n-Me2C=C(Me)CH2PdClJ2 + Ars in CDC13 at low temp. was detected by NMR spectroscopy.
IR spectrum of the complex was recorded (972). [Cu(Ars)Cl], crystals, prepd. from CU2C12 and the arsine in CHC~, recrystd. from CHC13-EtOH. The compn. of the crude prod. before recrystn. corresponded to the Cu(Ars)2Cl formula (972). [Cu(Ars)2CN], m. 179-181°, prepd. 2:10) by heating in a sealed tube at 150°. as postulated (382). [Au(Ars)C13], pale yellow crystals, prepd. from HAuC13 and the arsine and from AuC13 and PhGAuS (851). [(Ars)AuMn(CO)5], m. 2, prepd. from Au(Ars)Cl and Na[Mn(CO)5] in THF, stable in air and to moisture (832).
From AsC13 in Et20 by adding dropwise to 4-Me2NCloHeMgBr in Et20 under reflux, 35% yield (1519). 339-342° (1519). Rxn. with: AgCl04 in CeRs ~ a gray-colored soln. (1519). 2 UNSYMMETRIC R2R'As DERIVATIVES The methods of synthesis of the were summarized in the main volume were described. Secondary arsines alkali metal derivatives have been in the preparation of the arsines. unsymmetric arsines reported through 1964 (M-33).