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By Adorno Theodor W

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A schematic of this behaviour is shown in Figure 11. BPDA-PDA polyimide on Si-wafer, for example, is a material pair that would fall onto the ACTE-0 line, while some epoxies are at the ACTE>>O, which is one reason why a silica filled epoxy was chosen as the backing material (or superlayer) for the MELT samples [60]. There is some concern about the need for cooling the samples down to liquid nitrogen temperature, as the lower temperature may be below the ductile-brittle failure transition with some materials.

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The film thickness was determined by the x-ray fluorescence technique (Fischerscope X-RAY 1020). 02 was achieved by careful calibration and a counting time of 5 minutes. 4 g/cm3 was used for TiN films [lo]. 2 [13]. 57 Testing the adhesion of hard coatings The method yields in addition to the film modulus also Young's modulus of the substrate. A description of the laser acoustic method is given in more details elsewhere [6]. 3. 6 pm deposited on steel and for the pure substrate as well. The upper frequency limit is about 70 MHz.

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